서지주요정보
Al-0.5wt.%Cu 박막의 결정립성장과 Si 첨가 효과 = Grain growth of thin films of an Al-0.5WT.%Cu alloy and the effect of Si addition
서명 / 저자 Al-0.5wt.%Cu 박막의 결정립성장과 Si 첨가 효과 = Grain growth of thin films of an Al-0.5WT.%Cu alloy and the effect of Si addition / 박권식.
발행사항 [대전 : 한국과학기술원, 1993].
Online Access 제한공개(로그인 후 원문보기 가능)원문

소장정보

등록번호

8004134

소장위치/청구기호

학술문화관(문화관) 보존서고

MMS 93024

휴대폰 전송

도서상태

이용가능(대출불가)

사유안내

반납예정일

리뷰정보

초록정보

The grain growth of thin films of an A1-0.5wt.\%Cu and of an Al-0.5wt.\%Cu-1.0wt.\%Si alloys has been investigated primarily using transmission electron microscopy and X-ray diffraction. Thin films of 1$\mu$m were deposited on the thermally oxidized (100) Si wafer by sputtering technique. These films have been annealed in air-atmosphere for various times at various annealing temperatures. The variations of grain size distribution, mean grain diameter, and standared deviation were measured as function of annealing conditions. Digitized tablet linked with an IBM-PC was used to analyze the grain structures observed in TEM micrographs of plan view. The degree of the preferred orientation was measured using XRD and TEM. Relative peak intensity of $I_{111}$/$I_{200}$ was taken as the measure of the degree of the preferred orientation. In addition, the analysis of selectied area diffraction patterns has also been perfromed in order to directly measure the orientation of the grains. The average grain size of Al-0.5wt.\%Cu thin films in as-deposit condition was measured to be 0.65$\mu$m and its stadnard deviation was measured to be 0.22. Strong (111) preferred orientation was observed from the as-deposit condition. In the case of Al-0.5wt.\%Cu-1.0wt.\%Si thin films, the average grain size was measured to be 0.36$\mu$m, which is distinctively smaller than that in the Al-0.5wt.\%Cu thin films. Standard deviation 0.11 was also distinctively smaller. This is believed to be due to the formation of Si nodules during the deposition. Lesser pronounced (111) texture was observed in the case of an Al-0.5wt.\%Cu-1.0wt.\%Si thin films. The annealing treatment tend to increase the degree of the preferred orientation. In both thin films, the grain growth does not occur until the annealing temperature reaches $\sim 300^\circ C$. A rapid grain growth is observed within 15 minutes of annealing at temperature above $\sim 300^\circ C$. The grain growth proceeds very slowly afterwards. The coccurrence of grain growth above $\sim 300^\circ C$ is believed to be partly related with the dissolution of $Al_2Cu$ precipitates above this temperature. The transition of growth rate at $\sim$15min. could be due to the transition of the mode from 3-dimensional to 2-dimensional grain growth. In the case of an Al-0.5\%Cu-1.0\%Si thin films, a secondary rapid grain growth occurs at a later stage of annealing at above $\sim 500^\circ C$. This is believed to be due to the dissolution of Si precipitates at above $\sim 500^\circ C$. The application of Vaiyda's microstrucural model suggests that the annealing of an Al-0.5wt.\%Cu thin film at $500^\circ C$ reduces the resistance to the electromigration by 1/10 to that of as-deposit condition. In the case of an Al-0.5\%Cu-1.0\%Si thin film, the model predicts that reduces the resistance to the electromigration by the annealing at $500^\circ C$ 1/20 to that of as-deposit condition. This is due to a larger influence of the variation of the standard deviation as compared to that of the average grain size.

서지기타정보

서지기타정보
청구기호 {MMS 93024
형태사항 iv, 62 p. : 삽화, 사진 ; 26 cm
언어 한국어
일반주기 저자명의 영문표기 : Kwon-Shik Park
지도교수의 한글표기 : 박중근
지도교수의 영문표기 : Joong-Keun Park
학위논문 학위논문(석사) - 한국과학기술원 : 재료공학과,
서지주기 참고문헌 : p. 60-62
주제 Thin films.
Metal crystals --Growth.
Aluminum-copper alloys.
금속 박막. --과학기술용어시소러스
결정립 성장. --과학기술용어시소러스
첨가물 효과. --과학기술용어시소러스
알루미늄 합금. --과학기술용어시소러스
QR CODE

책소개

전체보기

목차

전체보기

이 주제의 인기대출도서